Multifaceted Characterization Research Articles

Influence of fluoride characteristics on tooth surface protection in an erosive condition: A multifaceted characterization approach.

To evaluate the effect of fluoride consistency and composition to protect enamel and dentin against the dental erosion. Bovine enamel and dentin specimens were treated with artificial saliva, neutral fluoride gel (NFG), acidulated phosphate fluoride gel (AFG), neutral fluoride foam (NFF), and acidulated phosphate fluoride foam. The samples were subjected to cycling. Micro energy-dispersive X-ray fluorescence spectrometry, surface roughness (Ra), contact angle (CA), and scanning electron microscopy (SEM) were performed. Composition, CA and Ra data were analyzed by ANOVA and multiple comparison test (p < 0.05). The dentin protected had a significantly higher mineral content than in the control. Eroded unprotected enamel had higher Ra values than normal surfaces. Fluoride treatments increased the Ra in dentin samples. AFG increased the CA in enamel. Fluoride foams increased CA in dentin with reduced mineral loss. SEM analysis found a deposited layer on enamel treated with AFG and remnants of deposits on dentin treated with NFG and NFF. Regardless of the form of application, fluoride provided protection against erosion, however with different levels. Applying the adequate fluoride form is relevant since the formulations have different effects on both enamel and dentin.

Adsorption of Cd(II) on mercapto-palygorskite functional materials with different proportions: Performance, mechanism and DFT study

Cd contamination has cosmopolitan harm and urgent needs to be addressed, the mercapto (-SH) modified materials are emerging in the Cd remediation field. In this study, three mercapto-palygorskite functional materials (0.2MP, 0.5MP, 1.0MP) were prepared by trimethoxysilane (MPTMS) and palygorskite (PAL) with different weight ratios (0.2:1, 0.5:1, 1:1), to investigate the effect of -SH proportions differences on material properties and combination configuration with Cd. The results indicated that mercapto groups grafting occurred on the PAL surface, retaining the original mineral structure. The adsorption capacity improved with the increase of -SH ratio, and 1.0MP (30.06 mg·g−1) was up to about 3 times of PAL (10.07 mg·g−1). The Cd stabilization subjected to the pseudo-second-order kinetic, Redlich-Paterson and Langmuir isothermal model, belonging to monolayer homogeneous chemisorption. Multifaceted characterization revealed that MP utilized mercapto and hydroxyl groups to form complexation with Cd as the dominant action mechanism. The electron transfer that took place from -SH to Cd was confirmed by Bader net change. DFT calculation manifested that bidentate complex S-Cd-S (Ead = −1.089 eV) was the best configuration of -SH combined with Cd due to its lower binding energy than the monodentate complex (Ead = −0.579 eV). This study confirms that MP as a friendly functional material offers a bright application prospect in the treatment of Cd contamination.

Green synthesis and multifaceted characterization of iron oxide nanoparticles derived from Senna bicapsularis for enhanced in vitro and in vivo biological investigation

Abstract Iron oxide nanoparticles have garnered significant interest in recent years due to their diverse applications, particularly in the therapeutic field. We present a green synthesis method using the extract of Senna bicapsularis, the production of iron oxide nanoparticles (IONPs). The successful synthesis of IONPs was confirmed by UV–visible spectroscopy, revealing the characteristic peak at 295 nm. Fourier-transform infrared spectroscopy (FTIR) and scanning electron microscopy were employed to elucidate the functional groups involved in the synthesis and characterize the morphological features of the nanoparticles. Subsequently, the synthesized IONPs were subjected to biological assays to assess their anticancer, enzyme inhibitory, analgesic, and sedative activities, following standardized protocols. The IONPs exhibited potent anticancer activity against the MDR 2780AD cell line, with IC50 values of 0.85 (extract) and 0.55 (iron oxide nanoparticles). Remarkable inhibitory effects were also observed against urease (IC50 = 12.98 ± 0.98) and xanthine oxidase (IC50 = 96.09 ± 0.65). Additionally, they demonstrated moderate carbonic anhydrase II inhibition, with 42.09% inhibition at a concentration of 0.25 mM. Furthermore, the extract and IONPs demonstrated a significant analgesic effect in a dose-dependent manner, while the sedative effect was also significant (p &lt; 0.001).

Biosynthesis and Multifaceted Characterization of Breynia nivosa-Derived Silver Nanoparticles: An Eco-Friendly Approach for Biomedical Applications.

This study presents an environmentally friendly synthesis of stable silver nanoparticles (Ag-NPs) using the methanolic extract of Breynia nivosa. Initial phytochemical analysis of the extract revealed the presence of alkaloids, flavonoids, glycosides, saponins, and tannins. Further characterization through high-performance liquid chromatography (HPLC) and gas chromatography-mass spectrometry (GC-MS) analyses identified a diverse array of bioactive compounds, including hydroquinone, stearic acid, neophytadiene, 9,12-octadecadienoic acid (Z,Z), methyl ester, and others. The addition of B. nivosa methanolic extract to an AgNO3 solution resulted in a color change, confirming the green synthesis of Ag-NPs through the reduction of AgNO3, as made evident by ultraviolet-visible (UV-vis) spectroscopy. X-ray diffraction (XRD) analysis provided valuable insights into the crystal structure, and scanning electron microscopy (SEM) analysis visualized the predominantly spherical shape of the Ag-NPs. However, the zeta (ζ)-potential and dynamic light scattering (DLS) analyses confirmed the stability and nanoscale dimensions of the synthesized Ag-NPs. Meanwhile, Fourier transform infrared (FT-IR) spectra exhibited peaks indicative of various functional groups, including carboxylic acids, phenols, alkanes, and isocyanates. These functional groups played a crucial role in both the reduction and capping processes of the Ag-NPs. The study further explored the antioxidant activity, cytotoxicity, acetylcholinesterase inhibition, and α-amylase inhibition activities of the Ag-NPs of the B. nivosa extract, demonstrating their potential for biomedical and therapeutic applications. In conclusion, this environmentally sustainable synthesis of Ag-NPs from the B. nivosa extract, enriched with bioactive secondary metabolites detected through HPLC and GC-MS analysis, holds promise for diverse applications in the burgeoning field of green nanotechnology.

Multifaceted Characterization for the Hepatic Clearance of Graphene Oxide and Size-Related Hepatic Toxicity.

Understanding the final fate of nanomaterials (NMs) in the liver is crucial for their safer application. As a representative two-dimensional (2D) soft nanomaterial, graphene oxide (GO) has shown to have high potential for applications in the biomedical field, including in biosensing, drug delivery, tissue engineering, therapeutics, etc. GO has been shown to accumulate in the liver after entering the body, and thus, understanding the GO-liver interaction will facilitate the development of safer bio-applications. In this study, the hepatic clearance of two types of PEGylated GOs with different lateral sizes (s-GOs: ~70 nm and l-GOs: ~300 nm) was carefully investigated. We found that GO sheets across the hepatic sinusoidal endothelium, which then may be taken up by the hepatocytes via the Disse space. The hepatocytes may degrade GO into dot-like particles, which may be excreted via the hepatobiliary route. In combination with ICP-MS, LA-ICP-MS, and synchrotron radiation FTIR techniques, we found that more s-GO sheets in the liver were prone to be cleared via hepatobiliary excretion than l-GO sheets. A Raman imaging analysis of ID/IG ratios further indicated that both s-GO and l-GO generated more defects in the liver. The liver microsomes may contribute to GO biotransformation into O-containing functional groups, which plays an important role in GO degradation and excretion. In particular, more small-sized GO sheets in the liver were more likely to be cleared via hepatobiliary excretion than l-GO sheets, and a greater clearance of s-GO will mitigate their hepatotoxicity. These results provide a better understanding of the hepatic clearance of soft NMs, which is important in the safer-by-design of GO.

NanoGuard: Antibacterial marvels of strontium titanate – Synthesis, characterization, and multifunctional insights

This study presents a comprehensive exploration into the synthesis and multifaceted characterization of strontium titanate (ST) nanopowder via the solution combustion method. The investigation delves into the photoluminescent properties, electrochemical behaviors assessed through potentiodynamic polarization (PDP) and electrochemical impedance spectroscopy (EIS), as well as antibacterial characteristics of the synthesized nanoproduct. Through meticulous analysis involving powder X-ray diffraction (PXRD), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), Fourier-transform infrared spectroscopy (FT-IR), and UV–visible spectroscopy (UV–vis), ST nanoparticles revealed intriguing features. PXRD unveiled a cubic crystal structure with a crystallite size of ∼ 11 nm, showcasing a crystallinity of 89.23. FESEM, UV–visible spectroscopy, and FT-IR studies uncovered irregularities in size, band gap properties, and the formation of M−O bonds within ST, with an Eg value of ∼ 3.0 eV. Photoluminescence investigations highlighted oxygen deficiencies within the ST material. Furthermore, corrosion inhibition efficiency was evaluated, demonstrating a maximum of 81.9 % at a concentration of 400 ppm, while antibacterial studies exhibited promising results against both Gram-positive (Bacillus subtilis) and Gram-negative (Escherichia coli) bacteria, with zone of inhibitions (ZOI) measuring 8.00 ± 0.250 mm and 9.00 ± 0.000 mm, respectively. These findings collectively underscore the diverse potential applications of ST nanoparticles and offer valuable insights into their structural, optical, electrochemical, and antimicrobial properties.

Antiacne Gel Containing Aloe vera and Clindamycin Phosphate: Design, Characterization, and Optimization Using Response Surface Methodology

Clindamycin phosphate is a topical antibiotic agent used to treat acne vulgaris, while Aloe vera has both antimicrobial and anti-inflammatory properties. The current study is aimed at formulating an antiacne gel with antioxidant and antimicrobial effects. The antiacne gels were prepared by using polymer HPMC K15M by cold dispersion method. Unveiling the intricacies of gel design, our research harnessed the power of Design Expert 11 to optimize critical parameters—viscosity, spreadability, and permeability. In vitro characterization tests, including pH, spreadability, viscosity, permeability, antimicrobial activity, antioxidant activity, and stability of the gels, were performed. The results of in vitro characterization tests showed that the gels had a mint-like odor, a pH of 6.8, and a spreadability of 21.5 g cm/sec. The gels had a viscosity of 34.2 Pa s and drug content ranging within 90%-110%, as per USP standards. Notably, in vitro permeation assays reveal an exceptional 86% drug release, showcasing the efficacy of our formulation. The uniqueness of our study lies not only in the robust optimization process but also in the multifaceted characterization. Our gel emerges as a promising candidate, exhibiting not only desired antimicrobial and antioxidant properties against acne vulgaris but also demonstrating stability under varied conditions. As we advance toward in vivo studies, our research paves the way for a nuanced understanding of the safety and efficacy of this distinctive antiacne gel.

3D Temperature-Controlled Interchangeable Pattern for Size-Selective Nanoparticle Capture.

Patterned surfaces with distinct regularity and structured arrangements have attracted great interest due to their extensive promising applications. Although colloidal patterning has conventionally been used to create such surfaces, herein, we introduce a novel 3D patterned poly(N-isopropylacrylamide) (PNIPAM) surface, synthesized by using a combination of colloidal templating and surface-initiated photoinduced electron transfer-reversible addition-fragmentation chain transfer (SI-PET-RAFT) polymerization. In order to investigate the temperature-driven 3D morphological variations at a lower critical solution temperature (LCST) of ∼32 °C, multifaceted characterization techniques were employed. Atomic force microscopy confirmed the morphological transformations at 20 and 40 °C, while water contact angle measurements, upon heating, revealed distinct trends, offering insights into the correlation between surface wettability and topography adaptations. Moreover, quartz crystal microbalance with dissipation monitoring and electrochemical measurements were employed to detect the topographical adjustments of the unique hollow capsule structure within the LCST. Tests using different sizes of PSNPs shed light on the size-selective capture-release potential of the patterned PNIPAM, accentuating its biomimetic open-close behavior. Notably, our approach negates the necessity for expensive proteins, harnessing temperature adjustments to facilitate the noninvasive and efficient reversible capture and release of nanostructures. This advancement hopes to pave the way for future innovative cellular analysis platforms.

Tabular Two-Dimensional Correlation Analysis for Multifaceted Characterization Data.

We propose tabular two-dimensional correlation spectroscopy analysis for extracting features from multifaceted characterization data, essential for understanding material properties. This method visualizes similarities and phase lags in structural parameter changes through heatmaps, combining hierarchical clustering and asynchronous correlations. We applied the proposed method to data sets of carbon nanotube (CNT) films annealed at various temperatures and revealed the complexity of their hierarchical structures, which include elements such as voids, bundles, and amorphous carbon. Our analysis addresses the challenge of attempting to understand the sequence of structural changes, especially in multifaceted characterization data where 11 structural parameters derived from eight characterization methods interact with complex behavior. The results show how phase lags (asynchronous changes from stimuli), and parameter similarities can illuminate the sequence of structural changes in materials, providing insights into phenomena such as the removal of amorphous carbon and graphitization in annealed CNTs. This approach is beneficial even with limited data and holds promise for a wide range of material analyses, demonstrating its potential in elucidating complex material behaviors and properties.

Are Aptamers Really Promising as Receptors for Analytical Purposes? Insights into Anti-Lysozyme DNA Aptamers through a Multitechnique Study.

Aptamers are recognition elements increasingly used for the development of biosensing strategies, especially in the detection of proteins or small molecule targets. Lysozyme, which is recognized as an important biomarker for various diseases and a major allergenic protein found in egg whites, is one of the main analytical targets of aptamer-based biosensors. However, since aptamer-based strategies can be prone to artifacts and data misinterpretation, rigorous strategies for multifaceted characterization of the aptamer-target interaction are needed. In this work, a multitechnique approach has been devised to get further insights into the binding performance of the anti-lysozyme DNA aptamers commonly used in the literature. To study molecular interactions between lysozyme and different anti-lysozyme DNA aptamers, measurements based on a magneto-electrochemical apta-assay, circular dichroism spectroscopy, fluorescence spectroscopy, and asymmetrical flow field-flow fractionation were performed. The reliability and versatility of the approach were proved by investigating a SELEX-selected RNA aptamer reported in the literature, that acts as a positive control. The results confirmed that an interaction in the low micromolar range is present in the investigated binding buffers, and the binding is not associated with a conformational change of either the protein or the DNA aptamer. The similar behavior of the anti-lysozyme DNA aptamers compared to that of randomized sequences and polythymine, used as negative controls, showed nonsequence-specific interactions. This study demonstrates that severe testing of aptamers resulting from SELEX selection is the unique way to push these biorecognition elements toward reliable and reproducible results in the analytical field.

Advantages of a Multifaceted Characterization of Honey, Illustrated with Irish Honey Marketed As Heather Honey

Advantages of a Multifaceted Characterization of Honey, Illustrated with Irish Honey Marketed As Heather Honey

Preparation and multifaceted characterization and optoelectronic potential of Cu/CuO/Cu2O nanoplates in a PVC/PE matrix

Preparation and multifaceted characterization and optoelectronic potential of Cu/CuO/Cu2O nanoplates in a PVC/PE matrix

Multifaceted Characterization and Thermal Stability of Y0.5Sr0.5Cr0.5Mn0.5O3 Chromite-Manganite Synthesized via Sol-Gel

Multifaceted Characterization and Thermal Stability of Y0.5Sr0.5Cr0.5Mn0.5O3 Chromite-Manganite Synthesized via Sol-Gel

Multifaceted Characterization of Human Embryonic Stem Cell-Derived Mesenchymal Stem/Stromal Cells Revealed Amelioration of Acute Liver Injury in NOD-SCID Mice.

Human embryonic stem cells (hESCs) are advantaged sources for large-scale and homogeneous mesenchymal stem/stromal cells (MSCs) generation. However, due to the limitations in high-efficiency procedures for hESC-MSCs induction, the systematic and detailed information of mesengenesis and early MSC development are largely obscure. In this study, we took advantage of the well-established twist-related protein 1 (TWIST1)-overexpressing hESCs and two small molecular cocktails (CHIR99021, decitabine) for high-efficient MSC induction. To assess the multidimensional biological and transcriptomic characteristics, we turned to cellular and molecular methods, such as flow cytometry (FCM), quantitative reverse transcription-polymerase chain reaction (qRT-PCR), in vitro tri-lineage differentiation, cytokine secretion analysis, in vivo transplantation for acute liver injury (ALI) management, and bioinformatics analyses (eg, gene ontology-biological processes [GO-BP], Kyoto Encyclopedia of Genes and Genomes [KEGG], HeatMap, and principal component analysis [PCA]). By combining TWIST1 overexpression (denoted as T) and the indicated small molecular cocktails (denoted as S), hESCs high-efficiently differentiated into MSCs (denoted as TS-MSCs, induced by T and S combination) within 2 weeks. TS-MSCs satisfied the criteria for MSC definition and revealed comparable tri-lineage differentiation potential and ameliorative efficacy upon ALI mice. According to RNA-sequencing (SEQ) analysis, we originally illuminated the gradual variations in gene expression pattern and the concomitant biofunctions of the programmed hESC-MSCs. Overall, our data indicated the feasibility of high-efficient generation of hESC-MSCs by TWIST1 and cocktail-based programming. The generated hESC-MSCs revealed multifaceted in vivo and in vitro biofunctions as adult BM-MSCs, which collectively suggested promising prospects in ALI management in future.

Uncovering the structural and photoelectric properties of perovskite crystals by joint multifaceted characterization and theoretical analysis

The potential of organic-inorganic hybrid perovskites, owing to their distinct photoelectric attributes and boosted photoluminescence stability, has garnered substantial attention. Despite comprehensive examinations of the synthesis and optical characteristics of FAPbBr3 crystals, the understanding of their microstructure's implication on photoelectric applications, their electronic configuration, and electron-phonon interplay remains vague. In this study, we detailed the electronic configuration, phonon dispersion, and vibrational properties using density functional theory. We further calculated the formation enthalpy stability diagram. Characterization and calculation of the crystalline structure were accomplished via Rietveld refinement. Phonon dispersion curves, as well as total and partial phonon densities of states, were also calculated. The theoretical results align well with experimental Fourier infrared and Raman spectra. Beyond elementary characterization, we explored the photoelectric qualities of FAPbBr3 crystals, thereby reaffirming the outstanding photoelectric attributes and extensive application potential. A non-contact fixed-point lighting device was designed based on the principle of electromagnetic induction coils, which proved the uniformity of crystal luminescence. According to the first principle, FAPbBr3 possesses a Poisson ratio of 0.32, indicative of high flexibility, emphasizing their superb photoelectric characteristics and vast application scope.

Ultrafast and simultaneous removal of four tetracyclines from aqueous solutions using waste material-derived graphene oxide-supported cobalt-iron magnetic nanocomposites.

In this work, a graphene oxide-supported cobalt-iron oxide (GO/Co-Fe) magnetic nanocomposite was successfully synthesized using waste dry cells for the efficient and simultaneous removal of tetracycline (TC), chlortetracycline (CTC), oxytetracycline (OTC), and doxycycline (DTC) from aqueous solutions. The GO/Co-Fe nanocomposite was thoroughly characterized using Fourier transform infrared spectroscopy, vibrating sample magnetometry, X-ray diffraction, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and zeta potential analysis. This multi-faceted characterization provided clean insights into the composition and properties of the synthesized nanocomposite. The adsorption of tetracyclines (TCs) was systematically investigated by assessing the influence of critical factors, such as adsorbent dosage, contact duration, initial pH of the solution, initial concentration, and temperature. The GO/Co-Fe adsorbent showed high removal efficiencies of 94.1% TC, 94.32% CTC, 94.22% OTC, and 96.94% DTC within 30 s contact period. The maximum removal efficiency of TCs was found at a low adsorbent dose of 0.15 g L-1. Notably, this superior removal efficiency was achieved at neutral pH and room temperature, demonstrating the adsorbent's efficacy under environmentally viable conditions. The kinetic studies demonstrated that the adsorption process was fitted satisfactorily with the pseudo-second-order model. Additionally, the adsorption behaviour of TCs on the GO/Co-Fe adsorbent was assessed by isotherm models, Langmuir and Freundlich. The experimental data followed the Langmuir isotherm, signifying a monolayer adsorption mechanism on the surface of the adsorbent. The adsorption capacities (qm) of GO/Co-Fe for TC, CTC, OTC and DTC were determined to be 64.10, 71.43, 72.46 and 99.01 mg g-1, respectively. Importantly, the GO/Co-Fe adsorbent showed reusability capabilities. The super magnetic properties of GO/Co-Fe made it easy to use for several cycles. These results clearly establish GO/Co-Fe as an exceptionally effective adsorbent for the removal of TCs from aqueous systems, highlighting its great potentiality in water treatment applications.

Synthesis, Characterization and Eco-friendly Applications of Biodegradable Polycaprolactone-Tapioca Starch Polymeric Composite Membrane

In the pursuit of sustainable materials, this study on the synthesis and multifaceted characterization of a novel biodegradable polymeric composite membrane. The polymeric composite composed of polycaprolactone (PCL) and tapioca starch (TS) was  meticulously prepared and it’s properties were systematically investigated. FTIR was employed to elucidate the structure of the  composite, while SEM facilitated the morphological examination. The biodegradability of the material was rigorously assessed through a burial method and a comparative analysis was also conducted against a commercially available facemask. The antimicrobial efficacy and the material’s suitability for water purification were also evaluated. The versatile application potential of the polymeric composite was further demonstrated through packaging tests utilizing tomatoes. The comprehensive investigated presented in this study demonstrates the advantageous sustain-ability of the PCL-TS polymer composite, hence highlighting its potential for many  environmental friendly applications. 

Złodzieje w międzywojennym Lublinie. Analiza historyczno-kryminologiczna

The article, the subject of which places it in the field of Urban Studies, is an attempt to present a multi-faceted characterization of the community of thieves in Lublin in the interwar period. For this purpose, methods of statistical and criminological analysis and GIS technology were used. First, the estimated size of the study group was determined. When reconstructing its characteristics, the influence of various variables (mainly sex and religion of the perpetrators of the theft) was taken into account. An initial description of the socio-professional structure of the environment was made. Thanks to the use of GIS technology, the local structure of the thieves’ place of residence and theft was reconstructed. By taking into account various variables, the pattern of criminal behaviour functioning in interwar Lublin was described. At the same time, the aggregation of the available data made it possible to construct a map of the then Lublin crime hotspots (i.e. areas characterized by a significant „concentration of pathological phenomena”). Finally, the author tried to answer the question of what motivated some of the then inhabitants of Lublin to resort to stealing. This is the first attempt to describe the spatial conditions of non-normative behaviour in the Second Polish Republic. Polish historiography of that period has not analysed the mutual relations between the nature of local criminal circles and the multidimensional specificity of the places where they functioned. Such research, mainly concerning the phenomenon of prostitution, is slowly becoming a standard in the historiography of Anglo-Saxon countries. The author hopes that the article will encourage similar studies to be undertaken in other cities of interwar Poland. The sum of such studies will make it possible to carry out broader analyses in the future, the results of which will complement the findings of Anglo-Saxon historiography.

Optimizing the Cell-Nanostructure Interface: Nanoconcave/Nanoconvex Device for Intracellular Recording of Cardiomyocytes.

Nanostructures are powerful components for the development of high-performance nanodevices. Revealing and understanding the cell-nanostructure interface are essential for improving and guiding nanodevice design for investigations of cell physiology. For intracellular electrophysiological detection, the cell-nanostructure interface significantly affects the quality of recorded intracellular action potentials and the application of nanodevices in cardiology research and pharmacological screening. Most of the current investigations of biointerfaces focus on nanovertical structures, and few involve nanoconcave structures. Here, we design both nanoconvex and nanoconcave devices to perform intracellular electrophysiological recordings. The amplitude, signal-to-noise ratio, duration, and repeatability of the recorded intracellular electrophysiological signals provide a multifaceted characterization of the cell-nanostructure interface. We demonstrate that devices based on both convex and concave nanostructures can create tight coupling, which facilitates high-quality and stable intracellular recordings and paves the way for precise electrophysiological study.

Structural Performance of Additively Manufactured Composite Lattice Structures: Strain Rate, Cell Geometry, and Weight Ratio Effects

The proliferation of ordered cellular structures in industrial and technological applications is justified by their superior mechanical performance, including tunable energy absorption strategies and potential multifunctionality. This research evaluates the mechanical response of composite lattice structures fabricated using vat photopolymerization additive manufacturing process and printable particulate composite materials. Several generations of modified printable resins are prepared by hybridizing flexible resin with varying glass microballoons reinforcement weight percentages. Multifaceted characterization regiments highlight the process–property–performance interrelationship by submitting printed composite structures to quasi‐static and impact‐loading scenarios combined with digital stills and high‐speed photography, respectively. Image analyses of optical and scanning electron micrographs quantify the dimensional accuracy of the composite lattice structures with cylindrical and hexagonal cellular geometries. The mechanical characterization uncovers the effect of cell geometry and reinforcement on the global structural behavior, eliciting differences in load‐bearing capacity, local strain developments, and structural densification. Exploratory digital image correlation supports the global structural deformations, revealing their relationship with the developed local strain state within the unit cells. The outcomes of this research elucidate the effect of strain rate, unit cell geometry, and reinforcing ratios on the structural performance of composite lattice structures at the macro‐ and microstructure levels.